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| Recent Posters using Total Error and Accuracy Profile approach : |
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| DEVELOPMENT AND VALIDATION OF A UPLC/MS/MS METHOD FOR THE ANALYSIS OF
OXYTETRACYCLINE IN NASAL SECRETIONS AND PLASMA OF HEALTHY PIGS |
M.A. Bimazubute1, E. Rozet2, J.-Cl. Van Heugen4, E. Arancio4, J. Crommen3, P. Gustin 1 and P. Chiap4
1. Unit of Pharmacology, Pharmacotherapy and Toxicology, Department for Functional Sciences, Faculty of Veterinary Medicine, B41, University of Liege, B-4000 Liege, Belgium
2. Laboratory of Analytical Chemistry and 3. Laboratory of Analytical Pharmaceutical Chemistry,
Bioanalytical Chemistry Research Unit, B36, University of Liege, B-4000 Liege, Belgium
4. Advanced Technology Corporation (A.T.C. s.a.), University Hospital Centre of Liege, B23, B-4000 Liege, Belgium |
| Place: HPLC 2007, Ghent, Belgium, June 17-21, 2007 |
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| LC DETERMINATION OF ENROFLOXACIN IN NASAL SECRETIONS AND PLASMA OF
HEALTHY PIGS USING RESTRICTED ACCESS MATERIAL FOR ON-LINE SAMPLE CLEAN-UP |
M.A. Bimazubute1, E. Rozet2, Ph. Hubert 2, P. Gustin 1, J. Crommen3 and P. Chiap4
1. Unit of Pharmacology, Pharmacotherapy and Toxicology, Department for Functional Sciences, Faculty of Veterinary Medicine, B41, University of Liege, B-4000 Liege, Belgium
2. Laboratory of Analytical Chemistry and 3. Laboratory of Analytical Pharmaceutical Chemistry,
Bioanalytical Chemistry Research Unit, B36, University of Liege, B-4000 Liege, Belgium
4. Advanced Technology Corporation (A.T.C. s.a.), University Hospital Centre of Liege, B23, B-4000 Liege, Belgium |
| Place: HPLC 2007, Ghent, Belgium, June 17-21, 2007 |
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| DEVELOPMENT AND PRE-VALIDATION OF A HIGH SENSITIVE METHOD FOR THE DETERMINATION OF LEVONORGESTREL IN HUMAN PLASMA BY SPE/LC/MS-MS |
C. Hubert1, B. Streel2, R. Sibenaler3, P. Chiap4 and Ph. Hubert1
1 Laboratory of Analytical Chemistry, Bioanalytical Chemistry Research Unit, Institute of Pharmacy, University of Liège, B36, 1, Av. de l’Hôpital, B-4000 Liège, Belgium
2 Galephar M/F s.a., 39, rue du Parc Industriel, B-6900 Marche-en-Famenne, Belgium
3 SMB Laboratories, 26-28, rue de la Pastorale, B-1080 Bruxelles, Belgium
4 Advance Technology Corporation (ATC), CHU, B35, 1, Av. de l’Hôpital, B-4000 Liège, Belgium |
| Place: HPLC 2007, Ghent, Belgium, June 17-21, 2007 |
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E-mail : chubert(at)ulg.ac.be
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| ENANTIOMERIC PURITY TESTING OF S-TIMOLOL BY NON-AQUEOUS CE USING HEPTAKIS(2,3-DI-O-METHYL-6-O-SULFO)-BETA-CYCLODEXTRIN AS CHIRAL ADDITIVE – VALIDATION USING THE ACCURACY PROFILE STRATEGY AND ESTIMATION OF UNCERTAINTY |
R. D. Marini, A.-C. Servais, E. Rozet, P. Chiap1, B. Boulanger2, S. Rudaz3, J. Crommen, Ph. Hubert, M. Fillet.
University of Liège, CHU, B 36, B-4000 Liège, Belgium
1 Advanced Technology Corporation, Liège, Belgium
2 UCB Pharma, Braine-L'Alleud, Belgium
3 University of Geneva, Geneva, Switzerland
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| Place: HPLC 2007, Ghent, Belgium, June 17-21, 2007 |
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| VALIDATION VERSUS ROUTINE: EVALUATION DE L’ASPECT PREDICTIF DE L'INTERVALLE DE TOLERANCE |
C. Hubert1, E. Rozet1, A. Ceccato2, W. Dewé2, E. Ziemons1, F. Moonen3, K. Michail4,5, R. Wintersteiger4, B. Streel6, B. Boulanger2 and Ph. Hubert1
1 Laboratoire de Chimie Analytique, Université de Liège, Belgique
2 Eli Lilly Development Center, Belgique
3 Arlenda s.a., Belgium
4 Institute of Pharmaceutical Sciences, University of Graz, Austria
5 Faculty of Pharmacy, University of Alexandria, Egypt
6 Galephar M/F s.a., Belgique |
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| Le point sur les drogues de synthèse émergentes : les pipérazines |
Y. Lecomte, O. Roussel, M. Perrin
Institut de Recherche Criminelle de la Gendarmerie Nationale
1, Boulevard Théophile Sueur - 93111 ROSNY-SOUS-BOIS Cedex - FRANCE
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| Place: SFTA - 15ème Congrès - PARIS |
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| Document : PPT version
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E-mail : ircgn(at)gendarmerie.defense.gouv.fr
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| Determination of the ionophoric coccidiostat monensin in chicken tissues by Liquid Chromatography-tandem Mass Spectrometry after withdrawal of medicated feed. |
E. Chéneau, J. Henri, Y. Pirotais, J.-P. Abjean, B. Roudaut , M. Laurentie and P. Sanders
AFSSA-Fougères - Community Reference Laboratory for Antimicrobial Residues in Food,
Laboratoire d’Etudes et de Recherches sur les Médicaments Vétérinaires et les Désinfectants, BP 90203, 35302 Fougères, France
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| Place: Fifth International Symposium on Hormone and Veterinary Drug Residue Analysis in Antwerp, Belgium, May 16-19, 2006 |
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| Evaluating measurement uncertainty for dioxins in routine analysis by the accuracy profile approach |
Gauthier Eppe1, Bruno Boulanger2, Philippe Hubert3, Marie-Louise Scippo4, Guy Maghuin-Rogister4 and Edwin De Pauw1
1 CART Mass Spectrometry Laboratory, Chemistry Department, University of Liège, Allée de la Chimie 3, B-6c Sart-Tilman, B-4000 Liège, Belgium
2 Lilly Development Centre, Statistical and Mathematical Sciences, rue Granbompré, 11, B-1348 Mont-Saitn-Guibert, Belgium
3 Department of Analytical Pharmaceutical Chemistry, Institute of Pharmacy, University of Liège, CHU, B36, B-4000 Liège 1, Belgium
4 CART Laboratory of Analysis of Foodstuffs of Animal Origin, University of Liège, Boulevard de Colonster B-43bis Sart-Tilman, B-4000 Liège, Belgium
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| Utilization of Accuracy Profiles as a Tool for the Validation of Analytical Methods |
A. Ceccato, P. Jacobs, A. Flament, M. Gibella and W. Dewé
Lilly Development Centre, B-1348 Mont-Saint-Guibert, Belgium |
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| transfert d’une methode de dosage automatisee de 3 catecholamines majeures dans l’urine humaine. |
E. Rozet1, R. Morello2, W. Dewe3, P. Chiap4, B. Boulanger3, K. S. Boos2, J. Crommen4 and Ph. Hubert1
1 Laboratory of Analytical Chemistry and 4 Laboratory of Analytical Pharmaceutical Chemistry, Bioanalytical Chemistry Research Unit, ULg, B 36, B-4000 Liège, Belgium.
2 Laboratory of BioSeparation, Institute of Clinical Chemistry, University Hospital Grosshadern, D-81366 Munich, Germany.
3 Lilly Development Centre, Statistical department, rue Granbompre, 11, B-1348 Mont-Saint-Guibert, Belgium. |
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| Transfer of a multidimensional on-line spe-lc-ecd method for the determination of three major catecholamines in native human urine. |
E. Rozet1, R. Morello2, W. Dewe3, P. Chiap4, B. Boulanger3, K. S. Boos2, J. Crommen4 and Ph. Hubert 1
1 Laboratory of Analytical Chemistry and 4 Laboratory of Analytical Pharmaceutical Chemistry, Bioanalytical Chemistry Research Unit, ULg, B 36, B-4000 Liège, Belgium.
2 Laboratory of BioSeparation, Institute of Clinical Chemistry, University Hospital Grosshadern, D-81366 Munich, Germany.
3 Lilly Development Centre, Statistical department, rue Granbompre, 11, B-1348 Mont-Saint-Guibert, Belgium. |
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| Towards a risk based methodology to assess the acceptability of an analytical method transfer: comparison of different approaches. |
E. Rozet1, W. Dewe2, B. Govaerts3, B. Boulanger2, A. Ceccato2, P. Chiap4, J. Crommen4 and Ph. Hubert1
1 Laboratory of Analytical Chemistry and 4 Laboratory of Analytical Pharmaceutical Chemistry, Bioanalytical Chemistry Research Unit, ULg, B 36, B-4000 Liège, Belgium.
2 Lilly Development Centre, rue Granbompre, 11, B-1348 Mont-Saint-Guibert, Belgium.
3 Institute of Statistics, Université Catholique de Louvain, 20, voie du Roman Pays, B-1348 Louvain-la-Neuve, Belgium. |
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| Use of accuracy profile for the validation of the direct quantitation of tagitinin c in tithonia diversifolia leaves by on-line coupling of supercritical co2 extraction to ft-ir spectroscopy by means of optical fibres |
E. Ziemons1, V. Barillaro2, E. Rozet1, N. Wandji Mbakop1, R. Lejeune1, L. Angenot3, L. Thunus1 and Ph. Hubert1
1 Laboratory of Analytical Chemistry, Bioanalytical Chemistry Research Unit, Department of Pharmacy, University of Liège, Avenue de l’Hôpital 1,Bât B36, 4000 Liège, Belgium.
2 Laboratory of Pharmaceutical Technology, Department of Pharmacy, University of Liège, Avenue de l’Hôpital 1, Bât B36, 4000 Liège, Belgium.
3 Laboratory of Pharmacognosy, Department of Pharmacy, University of Liège, Avenue de l’Hôpital 1, Bât B36, 4000 Liège, Belgium. |
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| Validation de méthodes analytiques : Recherche et dosage des stupéfiants dans le sang dans le cadre de la sécurité routière |
| Validation de méthodes analytiques : Recherche et dosage des stupéfiants dans le sang dans le cadre de la sécurité routière O. ROUSSEL*, S. HERVE, P. HERARD, O.MESSINES, M. PERRIN |
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E-mail : ircgn(at)gendarmerie.defense.gouv.fr
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